RT Journal Article SR Electronic A1 Strakosova, Angelina A1 Kratochvíl, Petr A1 Riedl, Jan A1 Průša, Filip T1 Phase and Mechanical Properties Response of the Mechanically Alloyed CoCrFeNiAlX High Entropy Alloys JF Manufacturing Technology Journal YR 2022 VO 22 IS 4 SP 471 OP 476 DO 10.21062/mft.2022.059 UL https://journalmt.com/artkey/mft-202204-0014.php AB The present work describes the influence of Al content on the CoCrFeNiAl high-entropy alloys pre-pared by the powder metallurgy technique. The preparation procedure consisted of mechanical alloy-ing and subsequent spark plasma sintering. The content of Al varied from 10 - 30 at.% which affected the microstructure and mechanical properties. Using scanning electron microscope (SEM) and X-ray diffraction analysis (XRD) was found the microstructure becomes more refined with increasing con-tent of Al accompanied by the annihilation of the ductile FCC solid solution (Cr0.25Fe0.25Co0.25Ni0.25) phase and growth of the brittle and hard BCC solid solution phase (α-Fe) and formation of Al(Co0.5Ni0.5) phases, improving the mechanical properties. The best combination of the porosity, hardness HV 30, and ultimate compressive strength (UCS) was achieved for the studied high-entropy alloy when it contained 20 at. % Al.